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README.md | 2 жил өмнө |
这次主要是要讲解除了大家熟悉的常规一维氢谱和碳谱以外,其他的一维核磁谱图,包括但不限于以下内容:
无氘代试剂的核磁实验
题目也可以用: 无氘代试剂核磁共振实验研究乙酰丙酮的酮-烯醇互变异构实验。
如果是这样子,就是突出“无氘代试剂”和“酮-烯醇互变异构实验”,这样子文章就是只需要做一个不同溶剂比例下的酮和烯醇的含量就可以了,就不需要那么多实验了。然后详细说明一下无氘代试剂和氘代试剂的区别,无氘代试剂的操作方案。
参考文献:mplified “No-D” NMR Methods for Routine Analysis and Organometallic Reagent Concentration Determination
No-deuterium proton NMR (No-D NMR): A simple, fast and powerful method for analyses of illegal drugs
No-D NMR (No-Deuterium Proton NMR) Spectroscopy: A Simple Yet Powerful Method for Analyzing Reaction and Reagent Solutions NMR Spectroscopy in Nondeuterated Solvents (No-D NMR): Applications in the Undergraduate Organic Laboratory
No-D quantitative 1H Nuclear Magnetic Resonance spectroscopy method for the determination of ethanol in distilled spirits
Quantification of cocaine and its adulterants by nuclear magnetic resonance spectroscopy without deuterated solvents (No-D qNMR)